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Cold mounting Consumables for perfect metallographic sample preparation

The term cold mounting covers all mounting methods that do not require the use of a hot mounting press. To create a optimal cold-mounted specimen, consider the following:

  • The specimen must not be affected or corroded by the resin selected for cold mounting
  • The specimen must be able to withstand the peak temperature of the mounting system.
  • To prevent gap formation, the specimen surface must be free of dust and grease before mounting, so that the specimen can be well wetted with the mounting medium.

QPREP cold mounting resins are available on methyl methacrylate or MMA-free and epoxy based. Acrylate or MMA-free based cold mounting resins are characterized by good removal rate, short curing times and good chemical resistance. Epoxy resins are used for mounting of porous and temperaturesensitive materials. Furthermore, they are used when the lowest possible gap formation is intended.


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How to cold mount with epoxy resin


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How to cold mount with acrylic resin

KEM 15 plus

QPREP KEM 15 PLUS is a universally applicable two-component cold mounting material based on a modified polyester resin. Due to its very low shrinkage, it is particularly suitable for boundary layer investigations.

Product Advantages

  • Very low shrinkage
  • High edge retention
  • Good chemical resistance
  • Good mechanical machinability
  • Easy dosage with enclosed measuring spoon
     
  • Curing temperature : ca. 85-100 °C
  • Curing time: ca. 25 min
  • Hardness (Shore D): 85
  • Removal rate: Very low

Recommended applications

  • Edge examination
  • Mounting of medium-hard to hard materials
  • Curing by means of overpressure with pressure equipment possible, to minimize porosity and increase edge retention

KEM 20

QPREP KEM 20 is a universally applicable two-component cold mounting material based on a methyl methacrylate resin compound. Transparent mountings can be realized when curing under overpressure.

Product Advantages

  • Feasibility of transparent mountings by means of pressure equipment
  • Good chemical resistance
  • Good mechanical machinability
  • Easy dosage with enclosed measuring spoon
     
  • Curing temperature : ca. 100-120 °C
  • Curing time: ca. 15 min
  • Hardness (Shore D): 84
  • Removal rate: medium

Recommended applications

  • Target preparations
  • Mounting of soft to medium-hard materials

KEM 30

QPREP KEM 30 is a universal two-component cold mounting resin based on a methyl methacrylate resin compound. It is a fast curing resin, which is particularly suitable for high sample throughput.
Product Advantages

  • Semi-transparent
  • Good chemical resistance
  • Good mechanical machinability
  • Easy dosage with enclosed measuring spoon
     
  • Curing temperature : ca. 95-110 °C
  • Curing time: ca. 5 min
  • Hardness (Shore D): 85
  • Removal rate: medium

Recommended applications

  • Routine testing with high sample throughput
  • Mounting of soft to medium-hard materials
  • Curing by means of overpressure with pressure equipment possible, to minimize porosity

KEM 35

QPREP KEM 35 is a universally applicable two-component cold mounting material based on a methyl methacrylate resin compound. Due to its very low shrinkage and hardness, it is particularly suitable for edge examination on materials with higher hardness.
Product Advantages

  • Very low shrinkage
  • High edge retention
  • Very good mechanical machinability
  • Easy dosage with enclosed measuring spoon
     
  • Curing temperature : ca. 85-110 °C
  • Curing time: ca. 12 min
  • Hardness (Shore D): 87
  • Removal rate: Very low

Recommended applications

  • Edge examination
  • Mounting of hard materials
  • Curing by means of overpressure with pressure equipment possible, to minimize porosity and increase edge retention

KEM 60

QPREP KEM 60 is a universally applicable, mineral-filled, MMA-free two-component cold mounting resin. It is characterized by short curing time and good mechanical machinability.
 

Product Advantages

  • Free of MMA
  • Good chemical resistance
  • Good mechanical machinability
     
  • Curing temperature : ca. 95-110 °C
  • Curing time: ca. 10 min
  • Hardness (Shore D): 85
  • Removal rate: low

Recommended applications

  • Routine mountings
  • Very wide range of application
  • Curing by means of overpressure with pressure equipment possible, to minimize porosity

QPREP SEM 5000

QPREP SEM 5000 is an electrically conductive cold mounting material based on a modified Methyl methacrylate compound. It is suitable for SEM examinations and electrolytic polishing.

Product Advantages

  • Electroconductive
  • Contains copper particles
     
  • Curing temperature : 85 - 110 °C
  • Curing time: 10 min
  • Hardness (Shore D): 91
  • Removal rate: Very low

Recommended applications

  • Scanning electron microscopy
  • Electrolytic polishing

QPOX 90

QPREP QPOX 90 is a transparent two-component cold mounting material based on an epoxy resin. Due to its good flowability, it is well suited for the pre-potting of specimens with filigree and complex geometries.

Product Advantages

  • Good transparency
  • Very low gap formation
  • Low viscosity
  • Suitable for vacuum infiltration
     
  • Curing temperature : RT to approx. 50 °C
  • Curing time: 16 - 24 hours
  • Hardness (Shore D): 79
  • Removal rate: high

Recommended applications

  • Routine mountings
  • Applicable for a wide range of materials
  • Target preparations
  • Infiltration of porous materials
  • Pre-potting of assembled printed circuit boards to fix electronic components prior to cutting.
  • Mounting of low hardness material

QPOX 92

QPREP QPOX 92 is a highly transparent two-component cold mounting material on epoxy resin. It is very well suited for specimens with filigree and complex geometries. In addition, QPOX 92 is particularly recommended for mounting materials with temperature sensitive surfaces and for target preparations.

Product Advantages

  • Very good transparency
  • Very low gap formation
  • Low viscosity
  • Suitable for vacuum infiltration
     
  • Curing temperature : RT to approx. 35 °C
  • Curing time: 12 - 13 hours (50% faster than QPOX 90)
  • Hardness (Shore D): 81
  • Removal rate: medium

Recommended applications

  • Routine mountings
  • Applicable for a wide range of materials
  • Target preparations of defects in coating surfaces
  • Infiltration of porous materials
  • Pre-potting of assembled printed circuit boards to fix electronic components prior to cutting.
  • Mounting of low hardness material

NEW: Qpox 94

Qpox 94 is a low-viscosity and transparent two-component epoxy-based cold mounting resin, ideal for samples with delicate and complex geometries. It is particularly suitable for sensitive and porous surfaces as well as target preparations. With a curing time of about 9 hours Qpox 94 allows transparent and gap-free mounting and preparation on the same day.

Product Advantages

  • Excellent adhesion and very low gap formation
  • Very good transparency
  • Low-bubble mountings
  • Low viscosity
     
  • Suitable for vacuum infiltration
  • Curing temperature: RT up to 45°C (Tmax = 100 to 140°C)
  • Curing time: 9 h at RT (25% faster than Qpox 92), 3 h at 45°C 
  • Hardness (Shore D): 80
  • Removal rate: High

Recommended applications

  • Low-gap and transparent preparations on the same day
  • Can be used for a wide range of materials
  • For vacuum infiltration of porous materials and material surfaces, such as metal foams, porous ceramic support material or samples with corrosion layers
  • Mountings and target preparations of assembled PCBs
  • For filigree and sensitive specimens of more complex geometries and low-hardness workpieces

Epoxy resins comparison chart

Vacuum infiltration and pressure device

When cold mounting porous specimens it is purposeful to infiltrate them under vacuum, with a low viscosity mounting medium (epoxy resins). The QPREP infiltration device offers a solution for mounting under vacuum.

For transparent cold mounting using methyl methacrylate, these must be cured in a pressure device under positive pressure (2 - 2.5 bar). This increases the boiling point of the mounting material and suppresses the formation of gas bubbles during polymerization. The QPREP Pressure unit is best suited for this purpose.

Product Advantages

  • Infiltration of porous materials
  • Reinforcement of fragile materials
  • Clear/transparent mounting possible with methyl methacrylate

Recommended applications

  • Infiltration device for mounting porous samples with epoxy resin (Qpox 90 / 92 / 94)
  • Pressure device for mounting with methyl methacrylate (KEM 15, 20, 30, 35, 60 and QPREP SEM 5000)

Cold mounting moulds

Choosing a cold mounting mould of the correct size and suitable material the result of the mounting can be optimized. QPREP offers a variety of reusable and chemically resistant moulds of different sizes and materials for this purpose.

Silicone rubber, round or rectangular, beveled edge

  • Flexibility of the material enables easy demoulding after curing
  • Thick-walled mould, therefore, not recommended for light curing
  • Without removable base

Polypropylene, round

  • Semi-transparent, therefore suitable for light curing
  • With removable base for easy demoulding after curing

Polyethylene, round

  • Opaque, therefore, not recommended for light curing
  • With removable base for easy demoulding after curing

PTFE, beveled edge, round

  • Long period of usage
  • High strength, for long shape retention
  • Opaque, therefore not recommended for light curing
  • With removable base for easy demoulding after curing

Accessories & tools for cold and UV mounting

The mixing of the different resin components as well as the exact positioning of your specimens influence the quality of your mounting. Therefore, QPREP supports with a wide range of tools and accessories for cold mounting. Mixing of the resin components, fixing and correct positioning of the samples in the cold mounting moulds can thus be realized reliably and safely.

Accessories

  • Mixing beakers and spatulas
  • Mounting utilities
  • Dosing spoons
  • Steel- and plastic clips

Perfect mounting – Instruments by QATM

Mounting is more reliable, safer and more efficient when performed with the right equipment: Knowledge, exercising care and the right choice of consumables and equipment are crucial.

Knowledge Base

If you would like to learn more about the different procedures, please visit our extensive Knowledge Base.

Our Knowledge Base article about mounting includes:

  • Advantages of materialographic mounting
  • The difference between cold and hot mounting
  • How to avoid gap formation between mounting compound and sample

Mixing of the compounds
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QATM Products & Contact

QATM offers a wide range of innovative machines for metallographic sample preparation. Accompanying QATM accessories and consumables are thoroughly tested and selected for perfect interaction with our machines. Contact us for a consultation, quote or to talk to one of our dedicated application specialists!

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